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  • The subfraction was eluted at t 46.1-46.5 min; 3.0 mg was further purified by RP-HPLC (gradient 0-60 min: 50-70% MeCN) to provide 5 (t 36.3 min, 1.6 mg) and 4 (t 38.9 min, 1.1 mg).
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