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  • Liquid Chromatography-quadrupole Time-of-flight Mass Spectrometry Measurements: The LC-QTOF-MS measurements were performed using an Agilent 1260 series LC binary pump and wellplate autosampler coupled to a 6520 accurate-mass Q-TOF LC-MS system equipped with a dual electrospray (ESI) ion source operated in negative-ion mode (Agilent Technologies, Santa Clara, CA).
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